Reflectoquant® Fixing Bath Test Strips, Catalog No. 16980/1
1. Method
Silver reacts with cadmium sulfide to form
brown-black silver sulfide, the concentration of which is determined
reflectometrically.
2. Measuring Range and Number of Determinations
| Measuring range1) |
Number of Determinations |
| 0.20 - 5.00g/l Ag |
50 |
1)for measurement of concentrations > 5.00g/l Ag, see section 6
3. Applications
Sample Material:
Fixing baths
4. Influence of Foreign Substances
This was checked - in the case of interfering
ions up to concentrations of 1,000mg/l - in solutions containing
1.5g/l and 0g/l Ag. The concentrations of foreign substances given in
the table lie below the limit at which the determination is interfered
with:
Concentrations of Foreign Substances in mg/l
or %
| Cu2+ |
100 |
S2- |
10 |
EDTA |
1,000 |
| Fe2+ |
10 |
SO3 |
1,000 |
NaCl |
10% |
| Fe3 |
10 |
SO52- |
1,000 |
Na2SO4 |
10% |
| Ni2+ |
100 |
S2O3 |
1,000 |
|
|
| Pb2+ |
1,000 |
|
|
|
|
5. Reagents and Auxiliaries
| The analytic test strips are stable at
least up to the date stated on the pack when stored in the closed
tube at +15 to +25°C. |
Package Contents:
Tube containing 50 analytical test strips Bar code strip
Other Reagents:
EM Quant® Fixing Bath Test, Cat.
No. 10008, measuring range 0.5-10 g/l Silver bromide, Cat. No. 1.19201, Merck, KGaA, Darmstadt, Germany
6. Preparation
- Check whether the silver content is within
the measuring range.
Use the EM Quant® Fixing Bath
Test as a guide. Samples containing more than 5.00g/l Ag must be
diluted with distilled water.
7. Procedure
- Observe the instructions for the RQflex Reflectometer.
The following applies to the Fixing Bath Test:
Measurement procedure A. Stored reaction
time: 30 sec.
- Remove 1 analytical test strip and immediately
reclose the tube.
- Press START button of the reflectometer and
at the same time immerse both reaction zones of the test
strip in the sample solution (10-30°C) for approx. 2 sec.
- Shake off excess liquid from the test strip
- As soon as the beeper sounds (5 sec. before
end of reaction time), insert the test strip all the way into the
strip adapter with the reaction zones facing the display.
- Read off the result from the display. The
result is automatically stored.
Notes:
- If the test strip is inserted into the
adapter after the reaction time has expired, renewed depression of
the START button will result in a false-high reading of the silver
concentration.
- At the end of each workday, cleanse the
strip adapter thoroughly with water or ethanol.
8. Method Control
To check analytical test strips, equipment and
procedure:
Dissolve 1.74g silver bromide in fresh fixing
bath solution, make up to 100ml, and mix.
Silver concentration
10g/l.
Dilute this standard solution to 1g/l silver
and analyze as described in section 7.
Purchase Fixing Bath (Silver) Test Strips 0.2-5.0 g/l Reflectoquant 1 PK *Requires RQflex 2 EMD# 16950-1
Gallade Part#: 16980-1
Mfr Part#: 16980-1
Brand: EMD Chemicals EM Science
Container: 1 PK of 50 Strips
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